Intramolecular cyclization of amido acids into pyrrolidinothieno(or [1]benzothieno)[3]azepinediones
Identifieur interne : 001299 ( France/Analysis ); précédent : 001298; suivant : 001300Intramolecular cyclization of amido acids into pyrrolidinothieno(or [1]benzothieno)[3]azepinediones
Auteurs : Mohamed Othman [France] ; Pierre Netchitailo [France] ; Bernard Decroix [France]Source :
- Journal of Heterocyclic Chemistry [ 0022-152X ] ; 1997-01.
Abstract
The synthesis of pyrrolidino[2,1‐b]thieno[3,2(2,3)‐f][3]azepinediones 7a,b and pyrrolidino[2,1‐b]‐[1]benzothieno[3,2(2,3)‐f][3]azepinediones 7c,d are described starting from thiophenes or [1]benzothio‐phenes acetic acids. Their selective reduction using triethylsilane led to the corresponding azepinones 17a‐d.
Url:
DOI: 10.1002/jhet.5570340134
Affiliations:
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